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This new edition of "Protecting Groups" by Philip Kocienski is a valuable addition to the synthetic chemist's bookshelf and will find an appreciative audience. It contains an enormous amount of valuable and highly organized information. It is beautifully and clearly written; a pleasure to read. The introductory chapter provides a sophisticated overview of the application of protecting groups in contemporary syntheses. At the heart of the book are seven chapters which deal authoritatively and thoroughly with the protection of the various core functional groups, from carbonyl to amino. The closing epilog rounds off the presentation with an insight into the realities of synthetic practice and twenty-five problems for people who love to understand chemistry. E. J. Corey
|DATE DE PUBLICATION||2004-Jan-01|
|TAILLE DU FICHIER||8,39 MB|
|NOM DE FICHIER||Protecting Groups.pdf|
The didactic presentation of the material makes this book an essential bench-top tool not only for specialists in organic chemistry, but also for students and all those involved in the preparation of organic molecules. Key Features: A critical survey of the most used protecting groups, as used by organic chemists Organization based on functional groups: hydroxyl ; diol; carbonyl; carboxyl ...
Chapter 3: Protecting Groups I. Protecting Groups of Hydroxyl Groups Consider the stability and effect of anomeric group! Consider the solubility of starting material (the choice of solvent)! Consider the reactivity of different hydroxyl groups! * DCM is common for pyranoses with 2-3 OH's. For pyranose with more than 4 OH's, use DMF or ...